(meso-tetra-p-tolylporphyrinato)Sn

Base Information

Chemical Name:(meso-tetra-p-tolylporphyrinato)Sn
CAS No.:129390-30-3
Molecular Formula:C₄₈H₃₆N₄Sn
Molecular Weight:787.551
Hs Code.:

Synonyms:(meso-tetra-p-tolylporphyrinato)Sn

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Chemical Property of (meso-tetra-p-tolylporphyrinato)Sn

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Technology Process of (meso-tetra-p-tolylporphyrinato)Sn

There total 6 articles about (meso-tetra-p-tolylporphyrinato)Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 26334-83-8
dichloro[5,10,15,20-tetrakis(p-tolyl)porphinato]tin(IV)

: 129390-30-3
(meso-tetra-p-tolylporphyrinato)Sn

Guidance literature:: With NaBEt₃H; In toluene; absence of air and moisture; stirring for 4 h; filtration, solvent removal (reduced pressure), dissoln. in PhMe, layering with hexanes, crystn. (-30°C, overnight), collection (filtration), drying (vac., room temp.);

Reference yield: 54.0%

: 5,10,15,20-tetrakis(4-methylphenyl)porphyrin

: tin(ll) chloride

: 129390-30-3
(meso-tetra-p-tolylporphyrinato)Sn

Guidance literature:: With pyridine; In tetrahydrofuran; (Ar); addn. of pyridine to soln. of compounds in presence of molecular sieves; refluxed for 6 h while stirred; reaction monitored by UV-vis spectroscopy;; filtration; evapn. (reduced pressure); chromy. (toluene, alumina); solvent removed; recrystn. (toluene/heptane 1/2); purity checked by (1)H NMR, UV-vis and IR spectroscopy;

Reference yield: 48.0%

: (TTP)Sn(NHtolyl)2

: 1636-34-6
2,3-diphenyl-2,3-butanediol

: 129390-30-3
(meso-tetra-p-tolylporphyrinato)Sn

: (TTP)Sn[OC(Me)(Ph)C(Me)(Ph)O]

Guidance literature:: In dichloromethane; under N2 atm. to soln. (TTP)Sn(NHtolyl)2 in CH2Cl2 soln. 2,3-diphenylbutane-2,3-diol in CH2Cl2 was added and stirred at room temp. for 40 min; solvent was removed in vacuo, residue was taken up in toluene, filtered andevapd., residue was redissolved in CH2Cl2, layered with hexane and placed in freezer at -25°C for 3 days, ppt. was filtered; elem. anal.;
DOI:10.1021/ic035123+