diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

Base Information

Chemical Name:diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate
CAS No.:1033780-39-0
Molecular Formula:C₃₅H₅₄NO₈P
Molecular Weight:647.789
Hs Code.:

Synonyms:diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

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Chemical Property of diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

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Technology Process of diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

There total 1 articles about diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1033780-38-9
4-hexadecyloxy-2-nitrobenzyl alcohol

: 28149-48-6
4-[(diethoxyphosphinyl)methyl]benzoic acid

: 1033780-39-0
diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/ja802407f

Reference yield: 70.0%

: 1033780-39-0
diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate

: 1033780-40-3
4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl)benzylphosphonic acid

Guidance literature:: diethyl 4-(4'-hexadecyloxy-2'-nitrobenzyloxycarbonyl) benzylphosphonate; With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 4h;

With water; In methanol; dichloromethane; for 1h; Further stages.; Acid hydrolysis;
DOI:10.1021/ja802407f