N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

Base Information

Chemical Name:N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide
CAS No.:1415992-41-4
Molecular Formula:C₁₄H₁₀BrF₂NO₂S₂
Molecular Weight:406.272
Hs Code.:

Synonyms:N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

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Chemical Property of N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

Chemical Property:

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Technology Process of N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

There total 3 articles about N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415992-40-3
N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzamide

: 1415992-41-4
N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

Guidance literature:: With tetraphosphorus decasulfide; In toluene; for 18h; Reflux;

Reference yield:

: 142994-04-5
2-fluoro-4-(methylsulphonyl)benzoic acid

: 1415992-41-4
N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 0 - 28 °C

2: pyridine / dichloromethane / 0.25 h / 25 - 28 °C / Inert atmosphere

3: tetraphosphorus decasulfide / toluene / 18 h / Reflux

With pyridine; tetraphosphorus decasulfide; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; toluene;

Reference yield:

: 2-fluoro-4-(methylsulphonyl)benzoyl chloride

: 1415992-41-4
N-(4-bromo-2-fluorophenyl)-2-fluoro-4-(methylsulfonyl)benzothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.25 h / 25 - 28 °C / Inert atmosphere

2: tetraphosphorus decasulfide / toluene / 18 h / Reflux

With pyridine; tetraphosphorus decasulfide; In dichloromethane; toluene;