C₃₆H₄₆N₄O₈S

Base Information

• Chemical Name: C₃₆H₄₆N₄O₈S
• CAS No.: 1613038-86-0
• Molecular Formula: C₃₆H₄₆N₄O₈S
• Molecular Weight: 694.849
• Mol file: 1613038-86-0.mol

Synonyms:C₃₆H₄₆N₄O₈S

Chemical Property of C₃₆H₄₆N₄O₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₆N₄O₈S

There total 7 articles about C₃₆H₄₆N₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C36H46N4O6S (1622244-99-8) → C36H46N4O8S (1613038-86-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;

DOI:10.1021/jo500771g

Reference yield:

C15H21IN2O3 (1613038-76-8) → C36H46N4O8S (1613038-86-0)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 8 h / 20 °C

2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C

3: lithium bromide / 4 h / 20 °C

4: sodium sulfide / methanol

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With sodium sulfide; copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; 1: |Sonogashira Cross-Coupling;

DOI:10.1021/jo500771g

Reference yield:

C18H23BrN2O3 (1613038-81-5) → C36H46N4O8S (1613038-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium sulfide / methanol

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With sodium sulfide; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;

DOI:10.1021/jo500771g

upstream raw materials:

C₁₅H₂₁IN₂O₃

C₁₈H₂₃BrN₂O₃

C₃₆H₄₆N₄O₆S

2-iodobenzylamine