2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone

Base Information

• Chemical Name: 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone
• CAS No.: 5155-60-2
• Molecular Formula: C₁₆H₁₆O₄
• Molecular Weight: 272.301

Synonyms:2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone

Chemical Property of 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone

Chemical Property:

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Technology Process of 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone

There total 2 articles about 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[1-Bromo-2-(2-methoxy-phenoxy)-ethyl]-2-methoxy-phenol → 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone (5155-60-2)

Guidance literature:

With bicarbonate; In dichloromethane; for 0.00833333h;

DOI:10.1021/jo00139a020

Reference yield:

1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)ethanol (7382-68-5) → 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone (5155-60-2)

Guidance literature:

Multi-step reaction with 2 steps

1: HBr / CH₂Cl₂ / 0.17 h / Ambient temperature

2: bicarbonate / CH₂Cl₂ / 0.01 h

With bicarbonate; hydrogen bromide; In dichloromethane;

DOI:10.1021/jo00139a020

Reference yield: 50.0%

10-methoxy-10H-anthracen-9-one (14629-83-5) + 2-Methoxy-4-[2-(2-methoxy-phenoxy)-eth-(Z)-ylidene]-cyclohexa-2,5-dienone (5155-60-2) → 1-(3-methoxy-4-hydroxyphenyl)-1-(10-methoxy-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)ethane (82247-24-3)

Guidance literature:

In water; at 45 ℃;

DOI:10.1021/jo00139a020

upstream raw materials:

1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)ethanol

Downstream raw materials:

1-(3-methoxy-4-hydroxyphenyl)-1-(10-methoxy-9-oxoanthracen-10-yl)-2-(2-methoxyphenoxy)ethane

10-Hydroxy-10-[1-(4-hydroxy-3-methoxy-phenyl)-2-(2-methoxy-phenoxy)-ethyl]-10H-anthracen-9-one

10-[1-(4-Hydroxy-3-methoxy-phenyl)-2-(2-methoxy-phenoxy)-ethyl]-10H-anthracen-9-one

1-(4-Acetoxy-3-methoxy-phenyl)-2-(2-methoxy-phenoxy)-ethan-1-sulfonsaeuremethylester

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