N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

Base Information

Chemical Name:N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride
CAS No.:79664-26-9
Molecular Formula:C₂₂H₄₆N₄*4ClH
Molecular Weight:512.478
Hs Code.:

Synonyms:N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

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Chemical Property of N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

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Technology Process of N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

There total 2 articles about N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1111644-24-6
N,N'-bis[3-(cyclohexyl(2-nitrobenzenesulfonyl)amino)propyl]-N,N'-bis(2-nitrobenzenesulfonyl)butane-1,4-diamine

: 79664-26-9
N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

Guidance literature:: N,N'-bis[3-(cyclohexyl(2-nitrobenzenesulfonyl)amino)propyl]-N,N'-bis(2-nitrobenzenesulfonyl)butane-1,4-diamine; With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2008.10.071

Reference yield:

: 71-44-3
Spermine

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 79664-26-9
N,N'-bis[3-(cyclohexylamino)propyl]butane-1,4-diamine tetrahydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; Yield given. Multistep reaction; 1) 95percent EtOH, 15 h, 2) 95percent EtOH, 20 to 25 deg C, 1 to 3 atm, 72 h;
DOI:10.1021/jo00338a042