(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Base Information

Chemical Name:(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane
CAS No.:1331740-77-2
Molecular Formula:C₂₃H₃₁BrCl₂OSi
Molecular Weight:502.394
Hs Code.:

Synonyms:(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Suppliers and Price of (2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Chemical Property:

Purity/Quality:

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Technology Process of (2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

There total 5 articles about (2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1331740-76-1
2-(3-bromo-4-(triisopropylsilyloxy)phenyl)-1-(4-chlorophenyl)ethanol

: 1331740-77-2
(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/cmdc.201100145

Reference yield:

: 1331740-66-9
2-(3-bromo-4-(triisopropylsilyloxy)phenyl)ethanol

: 1331740-77-2
(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2: diethyl ether / 2 h / 20 °C

3: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

With thionyl chloride; Dess-Martin periodane; N,N-dimethyl-formamide; In diethyl ether; dichloromethane;
DOI:10.1002/cmdc.201100145

Reference yield:

: 1331740-65-8
methyl 2-(3-bromo-4-(triisopropylsilyloxy)phenyl)acetate

: 1331740-77-2
(2-bromo-4-(2-chloro-2-(4-chlorophenyl)ethyl)phenoxy)triisopropylsilylane

Guidance literature:: Multi-step reaction with 4 steps

1: lithium borohydride; Trimethyl borate / diethyl ether / 48 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

3: diethyl ether / 2 h / 20 °C

4: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

With lithium borohydride; thionyl chloride; Trimethyl borate; Dess-Martin periodane; N,N-dimethyl-formamide; In diethyl ether; dichloromethane;
DOI:10.1002/cmdc.201100145