8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Base Information

Chemical Name:8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine
CAS No.:1009639-12-6
Molecular Formula:C₃₂H₅₂N₆O₅Si₂
Molecular Weight:656.973
Hs Code.:

Synonyms:8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

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Chemical Property of 8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

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Technology Process of 8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

There total 6 articles about 8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1009639-10-4
N-(3,5-dimethylphenyl)acetohydroxamic acid

: 1009639-09-1
O⁶-(benzotriazol-1-yl)-3′,5′-di-O-(t-butyldimethylsilyl)-2′-deoxyguanosine

: 1009639-12-6
8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Guidance literature:: With caesium carbonate; In 1,2-dimethoxyethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200984

Reference yield:

: 68395-77-7
N-(3,5-dimethylphenyl)hydroxylamine

: 1009639-12-6
8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / diethyl ether / 0 °C

2: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; caesium carbonate; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1002/ejoc.201200984

Reference yield:

: 99-12-7
5-nitro-m-xylene

: 1009639-12-6
8-[acetyl(3,5-dimethylphenyl)amino]-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyguanosine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 0 °C

2: sodium hydrogencarbonate / diethyl ether / 0 °C

3: caesium carbonate / 1,2-dimethoxyethane / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; In 1,2-dimethoxyethane; diethyl ether; ethanol;
DOI:10.1002/ejoc.201200984