(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

Base Information

Chemical Name:(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate
CAS No.:116211-67-7
Molecular Formula:C₂₀H₂₄Cl₂O₇
Molecular Weight:447.312
Hs Code.:

Synonyms:(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

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Technology Process of (1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

There total 1 articles about (1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 650-51-1
sodium trichloroacetate

: 116211-65-5
cis-4-(2',3',4'-trimethoxyphenyl)cyclohex-3-ene-1,2-diol diacetate

: 2065-35-2
hexachlorocyclopropane

: 95127-11-0
2,3,4-trimethoxybiphenyl

: 116211-67-7
(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

Guidance literature:: In 1,1,2,2-tetrachloroethylene; diethylene glycol dimethyl ether; for 3h; Heating;
DOI:10.1021/jo00256a009

Reference yield: 98.0%

: 116211-67-7
(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

: 116211-73-5
(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>heptane-2,3-diol

Guidance literature:: With potassium carbonate; In methanol; for 1h; Ambient temperature;
DOI:10.1021/jo00256a009

Reference yield:

: 116211-67-7
(1α,2α,3α,6α)-7,7-dichloro-6-(2',3',4'-trimethoxyphenyl)-bicyclo<4.1.0>heptane-2,3-diol diacetate

: 116211-76-8
6-chloro-2-methoxy-5-(2',3',4'-trimethoxyphenyl)cyclohepta-2,4,6-trien-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

2: 76 percent / trifluoroacetic anhydride (TFAA), DMSO / CH₂Cl₂ / 2 h / -60 °C

3: 32 percent / K₂CO₃ / acetone / 4 h / Ambient temperature

With potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; In methanol; dichloromethane; acetone;
DOI:10.1021/jo00256a009