2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

Base Information

Chemical Name:2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine
CAS No.:1314787-75-1
Molecular Formula:C₁₃H₆BrF₄N₃
Molecular Weight:360.108
Hs Code.:

Synonyms:2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

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Chemical Property of 2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

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Technology Process of 2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

There total 1 articles about 2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1314787-74-0
C₁₃H₈F₄N₄

: 1314787-75-1
2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

Guidance literature:: C₁₃H₈F₄N₄; With sulfuric acid; sodium nitrite; In acetic acid; at 10 - 20 ℃; for 0.5h;

With hydrogen bromide; copper(I) bromide; In sulfuric acid; water; acetic acid; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield: 67.0%

: 1314787-75-1
2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

: (1R,5S,8s)-3-(3-methylisothiazol-5-yl)-3-azabicyclo[3.2.1]octan-8-amine

: 8-(4-fluoro-2-(trifluoromethyl)phenyl)-N-(3-(3-methylisothiazol-5-yl)-3-azabicyclo[3.2.1]octan-8-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-amine

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In 1,4-dioxane; at 150 ℃; for 0.5h; Microwave irradiation;

Reference yield: 15.0%

: 1185019-85-5
3-methoxy-4-(3-methyl-1H-1,2,4-triazol-1-yl)aniline

: 1314787-75-1
2-bromo-8-(4-fluoro-2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridine

: 1314786-35-0
8-[4-fluoro-2-(trifluoromethyl)phenyl]-N-[3-methoxy-4-(3-methyl-1H-1,2,4-triazol-1-yl)phenyl]-[1,2,4]triazolo[1,5-a]pyridin-2-amine

Guidance literature:: With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In tert-butyl alcohol; at 110 ℃; for 20h; Inert atmosphere;