2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine

Base Information

Chemical Name:2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine
CAS No.:1158054-91-1
Molecular Formula:C₂₉H₂₆FeNOP
Molecular Weight:491.352
Hs Code.:

Synonyms:2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine

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Chemical Property of 2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine

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Technology Process of 2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine

There total 1 articles about 2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 102-54-5,55404-68-7
ferrocene

: 1158054-27-3
2-bromo-6-[2-(diphenylphosphinoyl)ethyl]pyridine

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1158054-91-1
2-[2-(diphenylphosphinoyl)ethyl]-6-ferrocenylpyridine

Guidance literature:: With (CH₃)3CLi; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; pentane; (N2); addn. of (CH3)3CLi in pentane to ferrocene in THF at 273 K, stirring for 0.5 h, addn. of ZnCl2 in THF at 195 K, stirring for 1 h at room temp., addn. of palladium compd. in THF, addn. of pyridine deriv. in THF at 273 K, stirrring at 333 K for 24 h; addn. of water, concg., addn. of ethyl acetate, washing organic layer with water, aq. soln. of K2C2O4, water and brine, drying, concg., chromy. (silica, from CH2Cl2 to 5% methanol in CH2Cl2), elem. anal.;
DOI:10.1021/om9000378