5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

Base Information

Chemical Name:5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne
CAS No.:204520-61-6
Molecular Formula:C₂₈H₂₆N₂
Molecular Weight:390.528
Hs Code.:

5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1<sup>(12)</sup>,13,15-triene-2,10-diyne

Synonyms:5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

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Chemical Property of 5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

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Technology Process of 5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

There total 5 articles about 5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 116510-22-6
1,2-bis(1-methylsulfonyloxyprop-1-yn-1-yl)benzene

: 140-28-3,87170-83-0
N,N'-Dibenzylethylenediamine

: 204520-61-6
5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1039/b000963f

Reference yield:

: 583-53-9
2,3-dibromobenzene

: 204520-61-6
5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / n-BuNH₂ / Pd(PPh₃)4 / various solvent(s) / 20 h / Heating

2: 85 percent / Et₃N / CH₂Cl₂ / 0.25 h / 20 °C

3: 72 percent / K₂CO₃ / dimethylformamide / 3 h / 20 °C

With potassium carbonate; N-butylamine; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; N,N-dimethyl-formamide; 1: Alkylation / 2: Substitution / 3: Cyclization;
DOI:10.1039/b000963f

Reference yield:

: 116510-02-2
1,2-bis(3-hydroxyprop-1-yn-1-yl)benzene

: 204520-61-6
5,8-dibenzyl-5,8-diazabicyclo[10.4.0]hexadeca-1⁽¹²⁾,13,15-triene-2,10-diyne

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / 0.25 h / 0 °C

2: K₂CO₃ / dimethylformamide

With potassium carbonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)10856-5