C₁₃H₁₃F₃N₂O₃

Base Information

Chemical Name:C₁₃H₁₃F₃N₂O₃
CAS No.:1227306-92-4
Molecular Formula:C₁₃H₁₃F₃N₂O₃
Molecular Weight:302.253
Hs Code.:

C<sub>13</sub>H<sub>13</sub>F<sub>3</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₃H₁₃F₃N₂O₃

Suppliers and Price of C₁₃H₁₃F₃N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₃F₃N₂O₃

Chemical Property:

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Technology Process of C₁₃H₁₃F₃N₂O₃

There total 6 articles about C₁₃H₁₃F₃N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: C₁₆H₁₇F₃N₂O₃

: 1227306-92-4
C₁₃H₁₃F₃N₂O₃

Guidance literature:: With oxygen; ozone; In methanol; dichloromethane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ml300209g

Reference yield:

: 1227306-91-3
C₁₆H₁₉F₃N₂O₂

: 1227306-92-4
C₁₃H₁₃F₃N₂O₃

Guidance literature:: C₁₆H₁₉F₃N₂O₂; With ozone; In methanol; dichloromethane; at -78 ℃; for 1h;

With dimethylsulfide; In methanol; dichloromethane;

Reference yield:

: 1227306-88-8
C₂₂H₃₄F₃NO₃Si

: 1227306-92-4
C₁₃H₁₃F₃N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2-chloropropionyl chloride / methanol / 20 °C / Inert atmosphere

2.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / tetrahydrofuran / 20 - 80 °C / Inert atmosphere

3.1: hydrazine hydrate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere; Acidic conditions

3.2: 80 °C

4.1: ozone; oxygen / methanol; dichloromethane / 1 h / -78 °C / Inert atmosphere

With hydrazine hydrate; 2-chloropropionyl chloride; tributylphosphine; oxygen; ozone; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; dichloromethane; 2.1: |Mitsunobu Displacement;
DOI:10.1021/ml300209g