cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

Base Information

• Chemical Name: cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester
• CAS No.: 475152-73-9
• Molecular Formula: C₁₄H₁₇NO₃S
• Molecular Weight: 279.36

Synonyms:cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

Chemical Property of cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

Chemical Property:

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Technology Process of cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

There total 1 articles about cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-acetyl-L-proline methyl ester (2311-25-3,18800-83-4,27460-51-1,114376-47-5) + thiophenol (108-98-5) → cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester (475152-73-9) + trans-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester

Guidance literature:

N-acetyl-L-proline methyl ester; With lithium perchlorate; acetic acid; In nitromethane; at 0 ℃; Electrolysis;

thiophenol; In nitromethane; at 20 ℃; for 16h; Further stages.;

DOI:10.1021/ol026713z

Reference yield:

cis-1-acetyl-5-phenylsulfanyl-pyrrolidine-2-carboxylic acid methyl ester (475152-73-9) → N-acetyl-L-proline methyl ester (2311-25-3,18800-83-4,27460-51-1,114376-47-5)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ol026713z

upstream raw materials:

N-acetyl-L-proline methyl ester

thiophenol

Downstream raw materials:

N-acetyl-L-proline methyl ester

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