10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Base Information

Chemical Name:10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid
CAS No.:220784-31-6
Molecular Formula:C₆₀H₆₆N₂O₈
Molecular Weight:943.193
Hs Code.:

Synonyms:10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Suppliers and Price of 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

There total 6 articles about 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 220784-30-5
allyl 10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoate

: 220784-31-6
10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00016a001

Reference yield:

: 1679-53-4
10-hydroxydecanoic acid

: 220784-31-6
10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h

2: 61 percent / mercury acetate / Heating

3: 67 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 1 h

4: 84 percent / dimedone, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / Ambient temperature

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; mercury(II) diacetate; pyridinium p-toluenesulfonate; dimedone; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00016a001

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 220784-31-6
10-<1'-<<(2''S,3''S,5''S)-2'',5''-bis<(fluorenylmethyloxycarbonyl)amino>-1'',5''-diphenylhex-3''-yl>oxy>ethoxy>decanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 84.2 percent / diisopropylethylamine / CH₂Cl₂ / Ambient temperature

2: 67 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 1 h

3: 84 percent / dimedone, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / Ambient temperature

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyridinium p-toluenesulfonate; dimedone; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00016a001