(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

Base Information

Chemical Name:(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine
CAS No.:932725-34-3
Molecular Formula:C₂₃H₂₃NO₃S
Molecular Weight:393.507
Hs Code.:

Synonyms:(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

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Technology Process of (S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

There total 8 articles about (S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1198161-47-5
C₂₃H₂₅NO₄S

: 932725-34-3
(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol9023453

Reference yield: 72.0%

: 1303530-22-4
N-(1-benzyl-2-hydroxyethyl)-N-(2-bromobenzyl)-4-methylbenzenesulfonamide

: 932725-34-3
(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 90 ℃; for 17h; Inert atmosphere;
DOI:10.1055/s-0030-1258406

Reference yield: 64.0%

: 932725-27-4
(S)-N-(2-hydroxy-benzyl)-N-(1-hydroxymethyl-2-phenyl-ethyl)-4-methyl-benzenesulfonamide

: 932725-34-3
(S)-3-benzyl-4-(toluene-4-sulfonyl)-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2009.10.126 DOI:10.1016/j.bmcl.2009.10.115