(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

Base Information

Chemical Name:(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate
CAS No.:1627963-68-1
Molecular Formula:C₃₇H₄₁NO₅S
Molecular Weight:611.802
Hs Code.:

Synonyms:(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

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Chemical Property of (E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

Chemical Property:

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Technology Process of (E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

There total 8 articles about (E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.9%

: 331948-76-6
4-formylphenyl thiophene-2-carboxylate

: 147622-38-6
4-n-dodecyloxybenzoic acid 4-aminophenyl ester

: 1627963-68-1
(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

Guidance literature:: In ethanol; for 0.166667h; Microwave irradiation;
DOI:10.1080/15421406.2013.858013

Reference yield:

: 5271-67-0
2-Thiophenecarbonyl chloride

: 1627963-68-1
(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / butanone / 4.5 h / 0 °C

2: ethanol / 0.17 h / Microwave irradiation

With triethylamine; In ethanol; butanone;
DOI:10.1080/15421406.2013.858013

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1627963-68-1
(E)-4-((4-(4-(dodecyloxy)benzoyloxy)phenylimino)methyl)phenyl thiophene-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 90 °C

2.1: water; potassium hydroxide / ethanol / 2 h / Reflux

3.1: dmap / dichloromethane / 0.17 h / 20 °C

3.2: 12 h

4.1: tin(ll) chloride / ethanol / 2 h / Reflux

5.1: ethanol / 0.17 h / Microwave irradiation

With dmap; water; potassium carbonate; tin(ll) chloride; potassium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/15421406.2013.858013