2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate

Base Information

• Chemical Name: 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate
• CAS No.: 1093203-08-7
• Molecular Formula: C₃₈H₅₀Cl₃NO₆Si
• Molecular Weight: 751.263

Synonyms:2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property of 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate

There total 1 articles about 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4-tri-O-benzyl-6-O-(triisopropylsilyl)-D-mannopyranose + trichloroacetonitrile (545-06-2) → 2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate (1093203-08-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1002/anie.200802161

Reference yield: 95.0%

2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate (1093203-08-7) + allyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranoside (640277-83-4) → allyl (2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl)-(1->2)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranoside (1093203-10-1)

Guidance literature:

2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate; allyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranoside; In diethyl ether; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

DOI:10.1002/anie.200802161

Reference yield: 90.0%

2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl trichloroacetimidate (1093203-08-7) + phenyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside → C69H76O13SSi

Guidance literature:

With eosin Y; diphenyldisulfane; In dichloromethane; at 20 ℃; Sealed tube; Irradiation;

DOI:10.1039/d1cc04887b

upstream raw materials:

trichloroacetonitrile

Downstream raw materials:

allyl (2,3,4-tri-O-benzyl-6-O-triisopropylsilyl-α-D-mannopyranosyl)-(1->2)-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1->6)-2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranoside

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