2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine

Base Information

• Chemical Name: 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine
• CAS No.: 113546-48-8
• Molecular Formula: C₂₄H₂₂N₆O₈S₂
• Molecular Weight: 586.606

Synonyms:2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine

Chemical Property of 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine

There total 3 articles about 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-chloro-N'-acetylurea (29376-04-3) + N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine (1050-82-4,43134-47-0,43134-48-1) → 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine (113546-48-8)

Guidance literature:

With triethylamine; In acetone; Ambient temperature;

Reference yield: 90.0%

acetic anhydride (108-24-7) + 2,5-bis(ureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine (113546-47-7) → 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine (113546-48-8)

Guidance literature:

With boron trifluoride diacetate; In acetic acid; 1.) 30 deg C, 10 min; 2.) reflux;

Reference yield:

2,5-bis(N'-acetylureido)-1,4-bis(benzenesulfonamido)benzene (113546-57-9) → 2,5-bis(N'-acetylureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine (113546-48-8)

Guidance literature:

With lead(IV) acetate; 1.) glacial acetic acid, 30 deg C, 1 h; 2.) glycerin, 10 min;

upstream raw materials:

N-chloro-N'-acetylurea

N,N'-bis(phenylsulfonyl)-p-benzoquinone diimine

acetic anhydride

2,5-bis(ureido)-N,N'-bis(phenylsulfonyl)-1,4-benzoquinonediimine

Downstream raw materials:

2,5-bis(N'-acetylureido)-1,4-bis(benzenesulfonamido)benzene

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