1-(5-CHLORO-2-METHOXYPHENYL)PIPERAZINE HYDROCHLORIDE

Base Information

• Chemical Name: 1-(5-CHLORO-2-METHOXYPHENYL)PIPERAZINE HYDROCHLORIDE
• CAS No.: 99857-72-4
• Molecular Formula: C11H16Cl2N2O
• Molecular Weight: 226.706
• Hs Code.: 2933599090
• Mol file: 99857-72-4.mol

Synonyms:1-(2-Methoxy-5-chlorophenyl)piperazine;1-(5-Chloro-2-methoxyphenyl)piperazine;4-(5-Chloro-2-methoxyphenyl)piperazine;

Chemical Property of 1-(5-CHLORO-2-METHOXYPHENYL)PIPERAZINE HYDROCHLORIDE

Chemical Property:

• Melting Point: 216 °C
• Boiling Point: 375.8 °C at 760 mmHg
• Flash Point: 181.1 °C
• PSA: 24.50000
• LogP: 2.95400

Purity/Quality:

97% ^*data from raw suppliers

1-(5-Chloro-2-methoxy-phenyl)-piperazinexHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38-36
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(5-CHLORO-2-METHOXYPHENYL)PIPERAZINE HYDROCHLORIDE

There total 1 articles about 1-(5-CHLORO-2-METHOXYPHENYL)PIPERAZINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-(5-chloro-2-methoxy-phenyl)-piperazine (99857-72-4)

Guidance literature:

Reference yield: 87.0%

1-(3-chloropropyl)-4-methyl-4-phenylpiperidine-2,6-dione (1312809-01-0) + 1-(5-chloro-2-methoxy-phenyl)-piperazine (99857-72-4) → 1-[3-[4-(5-chloro-2-methoxyphenyl)piperazin-1-yl]propyl]-4-methyl-4-phenylpiperidine-2,6-dione (1312809-20-3)

Guidance literature:

at 140 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2011.03.054

Reference yield: 87.0%

1-(3-chloropropyl)-4-phenylpiperidine-2,6-dione (1312808-94-8) + 1-(5-chloro-2-methoxy-phenyl)-piperazine (99857-72-4) → 1-[3-[4-(5-chloro-2-methoxyphenyl)piperazin-1-yl]propyl]-4-phenylpiperidine-2,6-dione (1312809-07-6)

Guidance literature:

at 140 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2011.03.054

Downstream raw materials:

2-{2-[4-(5-chloro-2-methoxy-phenyl)-piperazin-1-yl]-ethyl}-isoindole-1,3-dione

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