thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

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Chemical Name:thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside
CAS No.:1400810-13-0
Molecular Formula:C₄₀H₃₂F₄O₇S
Molecular Weight:732.749
Hs Code.:

Synonyms:thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

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Technology Process of thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

There total 1 articles about thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1070321-04-8
thiophenyl 3,6-di-O-benzyl-α-D-mannopyranoside

: 35730-09-7
2,5-difluorobenzoyl chloride

: 1400810-13-0
thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja307628w

Reference yield: 90.0%

: 1400810-12-9
benzyl 2-O-benzyl-4,6-O-(R)-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1400810-13-0
thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside

: 1400810-14-1
benzyl [3,6-di-O-benzyl-2,4-O-(2,5-difluorobenzoyl)-α-D-mannopyranosyl-(1→3)]-2-O-benzyl-4,6-O-(R)-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-Dglucopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: benzyl 2-O-benzyl-4,6-O-(R)-benzylidene-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside; thiophenyl 3,6-di-O-benzyl-2,4-di-O-(2,5-difluorobenzoyl)-α-D-mannopyranoside; In dichloromethane; toluene; at 20 ℃; for 3h; Inert atmosphere; Molecular sieve;

With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -50 - -20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja307628w