4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

Base Information

Chemical Name:4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine
CAS No.:123705-01-1
Molecular Formula:C₂₅H₂₉N₅O₄
Molecular Weight:463.536
Hs Code.:

Synonyms:4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

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Technology Process of 4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

There total 5 articles about 4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 123705-11-3
4,5-bis-(hydroxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

: 1795-48-8
Isopropyl isocyanate

: 123705-01-1
4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

Guidance literature:: With dmap; In dichloromethane; for 120h; Heating;
DOI:10.1002/jhet.5570260246

Reference yield:

: 116834-17-4
1-phenyl-5-(1-pyrryl)pyrazole-4-acetic acid

: 123705-01-1
4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / 96 percent H₂SO₄ / Heating

2: 90 percent / Na, EtOH / 20 h / Ambient temperature

3: 72 percent / P₂O₅ / benzene / 2.5 h / Heating

4: 61 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

5: 92 percent / 4-dimethylaminopyridine / CH₂Cl₂ / 120 h / Heating

With dmap; lithium aluminium tetrahydride; ethanol; sulfuric acid; sodium; phosphorus pentoxide; In diethyl ether; dichloromethane; benzene;
DOI:10.1002/jhet.5570260246

Reference yield:

: 123705-08-8
ethyl 1-phenyl-5-(1-pyrryl)pyrazole-4-acetate

: 123705-01-1
4,5-bis-(isopropylaminocarbonyloxymethyl)-1-phenyl-1H-pyrazolo<3,4-e>indolizine

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Na, EtOH / 20 h / Ambient temperature

2: 72 percent / P₂O₅ / benzene / 2.5 h / Heating

3: 61 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

4: 92 percent / 4-dimethylaminopyridine / CH₂Cl₂ / 120 h / Heating

With dmap; lithium aluminium tetrahydride; ethanol; sodium; phosphorus pentoxide; In diethyl ether; dichloromethane; benzene;
DOI:10.1002/jhet.5570260246