1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

Base Information

Chemical Name:1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea
CAS No.:1187976-34-6
Molecular Formula:C₂₃H₃₀N₂OS
Molecular Weight:382.57
Hs Code.:

Synonyms:1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

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Chemical Property of 1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

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Technology Process of 1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

There total 4 articles about 1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2-{3-[2-(3,5-dimethyl-phenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-thioureido}-ethyl acetate

: 1187976-34-6
1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 6h;

Reference yield:

: 29875-08-9
3,5-dimethylbenzyl magnesium chloride

: 1187976-34-6
1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / 20 °C

1.2: 2 h / 40 °C

2.1: chloroform / 2 h / Reflux

3.1: water; lithium hydroxide / tetrahydrofuran / 6 h / 20 °C

With water; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; chloroform; toluene;

Reference yield:

: 41828-13-1
5,6,7,8-tetrahydro-naphthalene-1-carbaldehyde

: 1187976-34-6
1-[2-(3,5-dimethylphenyl)-1-(5,6,7,8-tetrahydronaphthalen-1-yl)-ethyl]-3-(2-hydroxyethyl)-thiourea

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / 20 °C

1.2: 2 h / 40 °C

2.1: chloroform / 2 h / Reflux

3.1: water; lithium hydroxide / tetrahydrofuran / 6 h / 20 °C

With water; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; chloroform; toluene;