O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide

Base Information

• Chemical Name: O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide
• CAS No.: 99944-69-1
• Molecular Formula: C₁₉H₁₇BrO₆
• Molecular Weight: 421.244
• Mol file: 99944-69-1.mol

Synonyms:O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide

Chemical Property of O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide

There total 3 articles about O³,O⁵-dibenzoyl-α-D-ribofuranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-tri-O-benzoyl-α-D-ribofuranoside (22224-41-5) → O3,O5-dibenzoyl-α-D-ribofuranosyl bromide (99944-69-1)

Guidance literature:

With dichloromethane; hydrogen bromide;

DOI:10.1021/ja01635a060

Reference yield:

O2,O3,O5-Tribenzoyl-D-ribose (55797-81-4) → O3,O5-dibenzoyl-α-D-ribofuranosyl bromide (99944-69-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane; hydrogen bromide; acetic acid / Behandeln des nach der Hydrolyse erhaltenen Reaktionsprodukts mit wss. Aceton und anschliessend Behandeln mit wss. Natriumhydrogencarbonat-Loesung

2: dichloromethane; hydrogen bromide

With dichloromethane; hydrogen bromide; acetic acid;

DOI:10.1021/ja01635a060

Reference yield:

→ O3,O5-dibenzoyl-α-D-ribofuranosyl bromide (99944-69-1)

Guidance literature:

1,3,5-Tri-O-benzoyl-α-D-ribofuranose, HBr in CHCl3;

DOI:10.1139/v62-045

upstream raw materials:

1,3,5-tri-O-benzoyl-α-D-ribofuranoside

O²,O³,O⁵-Tribenzoyl-D-ribose

Downstream raw materials:

hydrogen bromide