S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

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Chemical Name:S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside
CAS No.:848397-71-7
Molecular Formula:C₃₃H₃₂O₇S₂
Molecular Weight:604.745
Hs Code.:

Synonyms:S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

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Chemical Property of S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

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Technology Process of S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

There total 1 articles about S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98-59-9
p-toluenesulfonyl chloride

: 158716-07-5
phenyl 3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 848397-71-7
S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

Guidance literature:: With sodium hydroxide; potassium carbonate; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2005.05.112

Reference yield: 85.0%

: 848397-71-7
S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside

: 3,6-di-O-benzyl-1,2-dideoxy-2-phenylthio-D-glucopyranose

Guidance literature:: S-phenyl 3-O-benzyl-4,6-O-benzylidene-2-O-(p-toluenesulfonyl)-α-D-thiomannopyranoside; With sodium cyanoborohydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 12h;
DOI:10.1016/j.tetasy.2004.11.032