C₁₃H₁₄FNO₂

Base Information

Chemical Name:C₁₃H₁₄FNO₂
CAS No.:1402585-15-2
Molecular Formula:C₁₃H₁₄FNO₂
Molecular Weight:235.258
Hs Code.:

C<sub>13</sub>H<sub>14</sub>FNO<sub>2</sub>

Synonyms:C₁₃H₁₄FNO₂

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Chemical Property of C₁₃H₁₄FNO₂

Chemical Property:

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Technology Process of C₁₃H₁₄FNO₂

There total 5 articles about C₁₃H₁₄FNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 557-21-1
zinc(II) cyanide

: 1402585-14-1
C₁₂H₁₄FIO₂

: 1402585-15-2
C₁₃H₁₄FNO₂

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dimethyl amine; zinc; at 120 ℃; for 15h; Inert atmosphere;

Reference yield:

: 1402585-12-9
C₁₂H₁₄FNO₄

: 1402585-15-2
C₁₃H₁₄FNO₂

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 2 h

2: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

3: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; dimethyl amine / 15 h / 120 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; dimethyl amine; potassium iodide; zinc; sodium nitrite; In methanol; water; acetonitrile;

Reference yield:

: 107-59-5
tert-Butyl chloroacetate

: 1402585-15-2
C₁₃H₁₄FNO₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 0.5 h / -20 - -10 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / methanol / 2 h

3: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 10 - 20 °C

4: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; zinc; dimethyl amine / 15 h / 120 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; dimethyl amine; potassium iodide; zinc; sodium nitrite; In 1-methyl-pyrrolidin-2-one; methanol; water; acetonitrile;