6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

Base Information

Chemical Name:6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride
CAS No.:1310575-44-0
Molecular Formula:C₂₁H₂₄N₂O₂
Molecular Weight:336.434
Hs Code.:

Synonyms:6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

Chemical Property:

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Technology Process of 6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

There total 4 articles about 6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 6-benzoxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

: 1310575-44-0
6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

Guidance literature:: With 5% Pd(II)/C(eggshell); hydrogen; In methanol; for 24h;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 6-benzyloxy-1-(3-methoxyphenyl)-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

: 1310575-44-0
6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 24 h / Reflux

2: 5% Pd(II)/C(eggshell); hydrogen / methanol / 24 h

With 5% Pd(II)/C(eggshell); hydrogen; potassium carbonate; In methanol; acetonitrile;
DOI:10.1016/j.ejmech.2011.03.048

Reference yield:

: 2436-15-9
NSC 73391

: 1310575-44-0
6-hydroxy-1-(3-methoxyphenyl)-2-propyl-2,3,4,9-tetrahydro-1H-β-carboline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 24 h / Reflux

1.2: Cooling

2.1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

3.1: potassium carbonate / acetonitrile / 24 h / Reflux

4.1: 5% Pd(II)/C(eggshell); hydrogen / methanol / 24 h

With lithium aluminium tetrahydride; 5% Pd(II)/C(eggshell); hydrogen; potassium carbonate; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/j.ejmech.2011.03.048