2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

Base Information

Chemical Name:2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose
CAS No.:1327260-14-9
Molecular Formula:C₃₀H₄₂O₁₀
Molecular Weight:562.657
Hs Code.:

Synonyms:2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

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Chemical Property of 2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

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Technology Process of 2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

There total 2 articles about 2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-acetyl-1,2,4-tri-O-methyl-α-D-glucopyranose

: 1327260-14-9
2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

Guidance literature:: With methanol; potassium carbonate; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2011.05.124

Reference yield:

: 81928-96-3
3-O-Acetyl-4,6-di-O-benzyl-D-galactal

: 1327260-14-9
2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0.5 h / 50 °C / Microwave irradiation; Inert atmosphere

2: methanol; potassium carbonate / 4 h / 20 °C

With methanol; aluminum (III) chloride; potassium carbonate; In dichloromethane;
DOI:10.1016/j.tet.2011.05.124

Reference yield: 54.0%

: 1327260-14-9
2-deoxy-3,4,6-tri-O-benzyl-α-D-lyxo-hexopyranosyl-(1->6)-3-hyroxy-1,2,4-tri-O-methyl-α-D-glucopyranose

: 81928-96-3
3-O-Acetyl-4,6-di-O-benzyl-D-galactal

: 1327260-15-0
C₅₂H₆₆O₁₅

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 50 ℃; for 1.33333h; optical yield given as %de; diastereoselective reaction; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.124