1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Base Information

Chemical Name:1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid
CAS No.:345935-96-8
Molecular Formula:C₁₈H₁₈N₂O₂S
Molecular Weight:326.419
Hs Code.:

Synonyms:1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Suppliers and Price of 1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

There total 3 articles about 1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 14491-02-2
2,2-dimethyl-3-phenyl-2H-azirine

: 76905-90-3
7-Methyl-thieno<2,3-c>pyridin-1,1-dioxid

: 3,3,5-Trimethyl-1-phenyl-3a,8b-dihydro-3H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

: 345935-96-8
1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Guidance literature:: In benzene; for 2h; Ambient temperature; Irradiation; Mercury High-pressure Lamp 2028 W;
DOI:10.1002/hlca.19830660330

Reference yield: 52.4%

: 86911-32-2
3a-Brom-1,1,5-trimethyl-3-phenyl-2,3,3a,8b-tetrahydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

: 345935-96-8
1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Guidance literature:: With sodium cyanide; In dimethyl sulfoxide; for 2h; Ambient temperature;
DOI:10.1002/hlca.19830660330

Reference yield:

: 86911-31-1
3a-Brom-1,1,5-trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

: 345935-96-8
1,1,5-Trimethyl-3-phenyl-3a,8b-dihydro-1H-pyrrolo<3',4':4,5>thieno<2,3-c>pyridin-4,4-dioxid

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / NaBH₃CN / acetic acid / 1.5 h / Ambient temperature

2: 52.4 percent / NaCN / dimethylsulfoxide / 2 h / Ambient temperature

With sodium cyanide; sodium cyanoborohydride; In acetic acid; dimethyl sulfoxide;
DOI:10.1002/hlca.19830660330