5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

Base Information

Chemical Name:5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole
CAS No.:1354030-27-5
Molecular Formula:C₂₂H₂₅Cl₂N₃OS
Molecular Weight:450.432
Hs Code.:

Synonyms:5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

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Chemical Property of 5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

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Technology Process of 5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

There total 6 articles about 5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1354030-26-4
5-(4-bromobutoxy)benzo[d]thiazole

: 839712-09-3
1-(2,3-dichlorophenyl)-1,4-diazepane hydrochloride

: 1354030-27-5
5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

Guidance literature:: 5-(4-bromobutoxy)benzo[d]thiazole; With sodium iodide; In acetonitrile; for 0.5h; Reflux;

1-(2,3-dichlorophenyl)-1,4-diazepane hydrochloride; With potassium carbonate; In acetonitrile; Reflux;

Reference yield:

: 7686-41-1
5-hydroxybenzothioazole

: 1354030-27-5
5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / ethanol / Reflux

2.1: sodium iodide / acetonitrile / 0.5 h / Reflux

2.2: Reflux

With potassium carbonate; sodium iodide; In ethanol; acetonitrile;

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 1354030-27-5
5-(4-(4-(2,3-dichlorophenyl)-1,4-diazepan-1-yl)butoxy)benzo[d]thiazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium nitrite; sulfuric acid / water / 0 - 5 °C

1.2: 0 - 50 °C

2.1: lithium aluminium tetrahydride / benzene; diethyl ether / Cooling; Reflux; Inert atmosphere

2.2: pH 6

3.1: boric acid / 6 h / Reflux

4.1: hydrogen iodide / 5 h / Reflux

5.1: potassium carbonate / ethanol / Reflux

6.1: sodium iodide / acetonitrile / 0.5 h / Reflux

6.2: Reflux

With lithium aluminium tetrahydride; sulfuric acid; hydrogen iodide; boric acid; potassium carbonate; sodium iodide; sodium nitrite; In diethyl ether; ethanol; water; acetonitrile; benzene;