BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇

Base Information

• Chemical Name: BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇
• CAS No.: 1283076-78-7
• Molecular Formula: C₂₆H₃₇BrN₄O₂
• Molecular Weight: 517.509
• Mol file: 1283076-78-7.mol

Synonyms:BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇

Chemical Property of BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇

There total 1 articles about BrC₆H₂(CH₂N(CH₃)2)2CCC₄H₂N₂(O)2C₈H₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-bromo-4-iodo-2,6-bis[(dimethylamino)methyl]benzene (312304-54-4) + 5-ethynyl-1-n-octyluracil (500360-66-7) → BrC6H2(CH2N(CH3)2)2CCC4H2N2(O)2C8H17 (1283076-78-7)

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine; In N,N-dimethyl-formamide; at 0 - 55 ℃; for 19h; Inert atmosphere; Darkness;

DOI:10.1016/j.jorganchem.2010.10.018

Reference yield: 97.0%

BrC6H2(CH2N(CH3)2)2CCC4H2N2(O)2C8H17 (1283076-78-7) → BrC6H2(CH2N(CH3)2)2C6H2N2O2C8H17 (1283076-79-8)

Guidance literature:

With silver nitrate; In acetone; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.10.018

upstream raw materials:

1-bromo-4-iodo-2,6-bis[(dimethylamino)methyl]benzene

5-ethynyl-1-n-octyluracil

Downstream raw materials:

BrC₆H₂(CH₂N(CH₃)2)2C₆H₂N₂O₂C₈H₁₇