10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

Base Information

• Chemical Name: 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester
• CAS No.: 51415-43-1
• Molecular Formula: C₂₃H₂₂ClN₃O₇S
• Molecular Weight: 519.963

Synonyms:10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

Chemical Property of 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

Chemical Property:

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Technology Process of 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

There total 2 articles about 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(6R)-3t-hydroxy-3c-methyl-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester (33627-13-3) → 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester (51415-43-1)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In benzene;

DOI:10.1021/ja00844a045

Reference yield:

→ 10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester (51415-43-1)

Guidance literature:

S-Oxid;

Reference yield:

10-chloro-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester (51415-43-1) → (6R)-3t-chloro-3c-methyl-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester (51546-66-8)

Guidance literature:

With triethylamine; In chloroform; Ambient temperature;

DOI:10.1021/ja00844a045

upstream raw materials:

(6R)-3t-hydroxy-3c-methyl-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester

Downstream raw materials:

10-acetoxy-6β-(2-phenoxy-acetylamino)-penicillanic acid 4-nitro-benzyl ester

(6R)-3t-acetoxy-3c-methyl-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester

(6R)-3-methyl-8-oxo-7c-(2-phenyl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-nitro-benzyl ester

(6R)-3t-chloro-3c-methyl-8-oxo-7t-(2-phenoxy-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]octane-2c-carboxylic acid 4-nitro-benzyl ester

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