5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

Base Information

Chemical Name:5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine
CAS No.:148493-98-5
Molecular Formula:C₃₈H₃₇N₃O₇
Molecular Weight:647.728
Hs Code.:

Synonyms:5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

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Technology Process of 5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

There total 8 articles about 5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 148493-97-4
N-benzoyldeoxy-5-methylisocytidine

: 148493-98-5
5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

Guidance literature:: With dmap; triethylamine; In pyridine; 40 deg C, 3,5 h, then rt., 1 h;
DOI:10.1002/hlca.19980810502

Reference yield: 56.0%

: 207981-29-1
N²-benzoyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-5-methylisocytidine 3'-O-(2-cyanoethyl phosphonate)

: 148493-98-5
5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

Guidance literature:: With potassium fluoride; In methanol; for 5h; Ambient temperature;
DOI:10.1002/hlca.19980810502

Reference yield:

: 15425-09-9
3,5'-cyclo-2'-deoxyguanosine

: 148493-98-5
5'-(dimethoxytrityl)-N-benzoyldeoxy-5-methylisocytidine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NH₃ / methanol / 4 h / 103 °C

2: 66 percent / pyridine, 4-(dimethylamino)pyridine, Et₃N / 0.75 h / Ambient temperature

3: 73 percent / 4-(dimethylamino)pyridine, Et₃N / pyridine / 40 deg C, 3,5 h, then rt., 1 h

With pyridine; dmap; ammonia; triethylamine; In pyridine; methanol;
DOI:10.1002/hlca.19980810502