Technology Process of C32H27FIN5O5
There total 10 articles about C32H27FIN5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver fluoride;
In
dichloromethane;
at 20 ℃;
for 3h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylsilyl trifluoromethanesulfonate / acetonitrile; toluene / 0 - 70 °C
2: silver nitrate / dichloromethane / 20 °C / Inert atmosphere
3: sodium hydride; 3-Hydroxypropionitrile / tetrahydrofuran / 0 - 20 °C
4: pyridine / 1 h / 0 °C
5: sodium iodide / acetone / Reflux
6: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 60 °C
7: silver fluoride / dichloromethane / 3 h / 20 °C / Cooling with ice
With
pyridine; trimethylsilyl trifluoromethanesulfonate; silver fluoride; sodium hydride; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-Hydroxypropionitrile; sodium iodide;
In
tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: silver nitrate / dichloromethane / 20 °C / Inert atmosphere
2: sodium hydride; 3-Hydroxypropionitrile / tetrahydrofuran / 0 - 20 °C
3: pyridine / 1 h / 0 °C
4: sodium iodide / acetone / Reflux
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 60 °C
6: silver fluoride / dichloromethane / 3 h / 20 °C / Cooling with ice
With
pyridine; silver fluoride; sodium hydride; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-Hydroxypropionitrile; sodium iodide;
In
tetrahydrofuran; dichloromethane; acetone;