C₂₄H₄₂O₅Si

Base Information

• Chemical Name: C₂₄H₄₂O₅Si
• CAS No.: 1000670-66-5
• Molecular Formula: C₂₄H₄₂O₅Si
• Molecular Weight: 438.68
• Mol file: 1000670-66-5.mol

Synonyms:C₂₄H₄₂O₅Si

Chemical Property of C₂₄H₄₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₄H₄₂O₅Si

There total 1 articles about C₂₄H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C41H59NO8SSi → C24H42O5Si (1000670-66-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

DOI:10.1055/s-2007-991049

Reference yield: 91.0%

C24H42O5Si (1000670-66-5) → C24H40O6Si (1000670-67-6)

Guidance literature:

C₂₄H₄₂O₅Si; With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃;

With sodium chlorite; sodium dihydrogenphosphate; In tert-butyl alcohol; Further stages.;

DOI:10.1055/s-2007-991049

Reference yield:

C24H42O5Si (1000670-66-5) → C28H43NO7Si (1000670-68-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -78 °C

1.2: 91 percent / NaClO₂; NaH₂PO₄ / 2-methyl-propan-2-ol

2.1: EDC; HOBt; i-Pr₂NEt

2.2: 70 percent / DAST; DBU; BrCCl₃ / CH₂Cl₂ / 0 °C

With oxalyl dichloride; benzotriazol-1-ol; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; 1.1: Swern oxidation reaction;

DOI:10.1055/s-2007-991049

Downstream raw materials:

C₂₄H₄₀O₆Si

C₂₈H₄₃NO₇Si