N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine

Base Information

• Chemical Name: N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine
• CAS No.: 1423156-66-4
• Molecular Formula: C₃₉H₃₅N₅O₇
• Molecular Weight: 685.736

Synonyms:N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine

Chemical Property of N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine

Chemical Property:

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Technology Process of N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine

There total 1 articles about N⁶-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

acetic anhydride (108-24-7) + N6-benzoyl-9-{3'-O-[(4,4'-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine (325683-88-3) → N6-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine (1423156-66-4)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1016/j.bmcl.2012.12.080

Reference yield: 90.0%

N6-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine (1423156-66-4) → N6-benzoyl-9-(2'-O-acetyl-α-L-threofuranosyl)adenine (1423156-67-5)

Guidance literature:

With trichloroacetic acid; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.bmcl.2012.12.080

Reference yield:

N6-benzoyl-9-{2'-O-acetyl-3'-O-[(4',4-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine (1423156-66-4) → C25H20N5O8P

Guidance literature:

Multi-step reaction with 2 steps

1: trichloroacetic acid / dichloromethane / 0.08 h / 20 °C

2: pyridine / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

With pyridine; trichloroacetic acid; In 1,4-dioxane; dichloromethane;

DOI:10.1016/j.bmcl.2012.12.080

upstream raw materials:

acetic anhydride

N⁶-benzoyl-9-{3'-O-[(4,4'-dimethoxytriphenyl)methyl]-α-L-threofuranosyl}adenine

Downstream raw materials:

N⁶-benzoyl-9-(2'-O-acetyl-α-L-threofuranosyl)adenine

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