C₃₀H₂₉N₃O₄

Base Information Edit

Chemical Name:C₃₀H₂₉N₃O₄
CAS No.:321172-68-3
Molecular Formula:C₃₀H₂₉N₃O₄
Molecular Weight:495.578
Hs Code.:
Mol file:321172-68-3.mol

C<sub>30</sub>H<sub>29</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₃₀H₂₉N₃O₄

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Chemical Property of C₃₀H₂₉N₃O₄ Edit

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Technology Process of C₃₀H₂₉N₃O₄

There total 26 articles about C₃₀H₂₉N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 321172-31-0
(1R,2R,3S,4R,7R)-3-Chloro-7-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid methyl ester

: 321172-68-3
C₃₀H₂₉N₃O₄

Guidance literature:: Multi-step reaction with 24 steps

1: 100 percent / tBuOOH; VO(acac)2 / benzene

2: 97 percent / 2,6-lutidine / CH₂Cl₂

3: 98 percent / tBuOK / benzene

4: methylaluminum bis(2,6-di-tert-butyl-4-methylphenoxide) / toluene / -20 °C

5: piperidine / methanol

6: 87 percent / TBAF / tetrahydrofuran

7: CrO₃; H₂SO₄ / acetone

8: toluene; acetonitrile / 90 °C

9: nBuLi / tetrahydrofuran / 65 °C

10: tBuOK

11: 75 percent / nBu₃SnH; AIBN / benzene / Heating

12: 100 percent / methanol

13: 94 percent / pyridine; DMAP / CH₂Cl₂

14: 94 percent / LiBH₄; LiBEt₃H / tetrahydrofuran

15: pyrrolidine / [Pd(PPh₃)4] / tetrahydrofuran

16: DIEA / acetonitrile / 60 °C

17: 62 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

18: 92 percent / pyridine; DMAP / CH₂Cl₂

19: 96 percent / HCO₂H

20: NEt₃ / tetrahydrofuran

21: NaBH₄; H₂O / tetrahydrofuran

22: PBu₃ / tetrahydrofuran

23: MCPBA / tetrahydrofuran

24: NEt₃ / tetrahydrofuran

With pyrrolidine; piperidine; pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; tert.-butylhydroperoxide; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; formic acid; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tributylphosphine; sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; potassium hexamethylsilazane; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; lithium triethylborohydride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; acetonitrile; benzene; 7: Jones' oxidation / 9: Horner-Emmons reaction / 12: Michael addition / 17: Michael addition;

Reference yield:

: 321172-27-4
(1R,2R,3R,4R,7R)-3-Chloro-7-dimethylsilanyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid methyl ester

: 321172-68-3
C₃₀H₂₉N₃O₄

Guidance literature:: Multi-step reaction with 25 steps

1: 53 percent / aq. H₂O₂; KF; KHCO₃ / tetrahydrofuran; methanol

2: 100 percent / tBuOOH; VO(acac)2 / benzene

3: 97 percent / 2,6-lutidine / CH₂Cl₂

4: 98 percent / tBuOK / benzene

5: methylaluminum bis(2,6-di-tert-butyl-4-methylphenoxide) / toluene / -20 °C

6: piperidine / methanol

7: 87 percent / TBAF / tetrahydrofuran

8: CrO₃; H₂SO₄ / acetone

9: toluene; acetonitrile / 90 °C

10: nBuLi / tetrahydrofuran / 65 °C

11: tBuOK

12: 75 percent / nBu₃SnH; AIBN / benzene / Heating

13: 100 percent / methanol

14: 94 percent / pyridine; DMAP / CH₂Cl₂

15: 94 percent / LiBH₄; LiBEt₃H / tetrahydrofuran

16: pyrrolidine / [Pd(PPh₃)4] / tetrahydrofuran

17: DIEA / acetonitrile / 60 °C

18: 62 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

19: 92 percent / pyridine; DMAP / CH₂Cl₂

20: 96 percent / HCO₂H

21: NEt₃ / tetrahydrofuran

22: NaBH₄; H₂O / tetrahydrofuran

23: PBu₃ / tetrahydrofuran

24: MCPBA / tetrahydrofuran

25: NEt₃ / tetrahydrofuran

With pyrrolidine; piperidine; pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; tert.-butylhydroperoxide; dmap; potassium fluoride; sodium tetrahydroborate; lithium borohydride; n-butyllithium; formic acid; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tributylphosphine; sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; tri-n-butyl-tin hydride; potassium hexamethylsilazane; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; lithium triethylborohydride; potassium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; acetonitrile; benzene; 8: Jones' oxidation / 10: Horner-Emmons reaction / 13: Michael addition / 18: Michael addition;

Reference yield:

: 321172-34-3
(1S,2R,4S,5R,6R,7S,8R)-7-Chloro-8-hydroxy-3-oxa-tricyclo[3.2.1.0^2,4]octane-6-carboxylic acid methyl ester

: 321172-68-3
C₃₀H₂₉N₃O₄

Guidance literature:: Multi-step reaction with 23 steps

1: 97 percent / 2,6-lutidine / CH₂Cl₂

2: 98 percent / tBuOK / benzene

3: methylaluminum bis(2,6-di-tert-butyl-4-methylphenoxide) / toluene / -20 °C

4: piperidine / methanol

5: 87 percent / TBAF / tetrahydrofuran

6: CrO₃; H₂SO₄ / acetone

7: toluene; acetonitrile / 90 °C

8: nBuLi / tetrahydrofuran / 65 °C

9: tBuOK

10: 75 percent / nBu₃SnH; AIBN / benzene / Heating

11: 100 percent / methanol

12: 94 percent / pyridine; DMAP / CH₂Cl₂

13: 94 percent / LiBH₄; LiBEt₃H / tetrahydrofuran

14: pyrrolidine / [Pd(PPh₃)4] / tetrahydrofuran

15: DIEA / acetonitrile / 60 °C

16: 62 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

17: 92 percent / pyridine; DMAP / CH₂Cl₂

18: 96 percent / HCO₂H

19: NEt₃ / tetrahydrofuran

20: NaBH₄; H₂O / tetrahydrofuran

21: PBu₃ / tetrahydrofuran

22: MCPBA / tetrahydrofuran

23: NEt₃ / tetrahydrofuran

With pyrrolidine; piperidine; pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; formic acid; 2,2'-azobis(isobutyronitrile); tributylphosphine; sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; potassium hexamethylsilazane; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; lithium triethylborohydride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; acetonitrile; benzene; 6: Jones' oxidation / 8: Horner-Emmons reaction / 11: Michael addition / 16: Michael addition;