C₂₃H₂₇NO₇

Base Information

Chemical Name:C₂₃H₂₇NO₇
CAS No.:1265278-73-6
Molecular Formula:C₂₃H₂₇NO₇
Molecular Weight:429.47
Hs Code.:

C<sub>23</sub>H<sub>27</sub>NO<sub>7</sub>

Synonyms:C₂₃H₂₇NO₇

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Chemical Property of C₂₃H₂₇NO₇

Chemical Property:

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Technology Process of C₂₃H₂₇NO₇

There total 21 articles about C₂₃H₂₇NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1265279-20-6
C₃₄H₅₃NO₇Si₂

: 1265278-73-6
C₂₃H₂₇NO₇

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 23 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201001281

Reference yield:

: 108534-61-8
(2-methoxyphenoxy)-(1,1-dimethylethyl)diphenylsilane

: 1265278-73-6
C₂₃H₂₇NO₇

Guidance literature:: Multi-step reaction with 20 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether; cyclohexane / 0.75 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

5.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

7.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

8.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

9.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

10.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

11.1: sodium tetrahydroborate / methanol / 1 h / 0 - 23 °C / Inert atmosphere

12.1: 1H-imidazole; dmap / dichloromethane / 16 h / 23 °C / Inert atmosphere

13.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

13.2: 16 h / 23 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

14.2: 3 h / -78 - 0 °C / Inert atmosphere

15.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

15.2: 4 h / -78 - 0 °C / Inert atmosphere

16.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

17.1: trimethylamine-N-oxide / tetrahydrofuran / 3 h / 23 - 70 °C / Inert atmosphere

18.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 23 °C

19.1: triethylamine; HATU / N,N-dimethyl-formamide / 14 h / 23 °C / Inert atmosphere

20.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

With 1H-imidazole; methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; 2-methyl-but-2-ene; Trimethyl borate; tributyl-amine; N,N,N,N,-tetramethylethylenediamine; trimethylamine-N-oxide; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; potassium hexamethylsilazane; potassium hydrogencarbonate; triethylamine; HATU; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; diethyl ether; decane; dichloromethane; cyclohexane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene; 2.1: Corey-Bakshi-Shibata reduction / 5.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281

Reference yield:

: 1048970-79-1
C₂₉H₃₄O₃Si

: 1265278-73-6
C₂₃H₂₇NO₇

Guidance literature:: Multi-step reaction with 19 steps

1.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

4.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

5.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

6.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

7.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

8.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

9.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

10.1: sodium tetrahydroborate / methanol / 1 h / 0 - 23 °C / Inert atmosphere

11.1: 1H-imidazole; dmap / dichloromethane / 16 h / 23 °C / Inert atmosphere

12.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

12.2: 16 h / 23 °C / Inert atmosphere

13.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

13.2: 3 h / -78 - 0 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

14.2: 4 h / -78 - 0 °C / Inert atmosphere

15.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

16.1: trimethylamine-N-oxide / tetrahydrofuran / 3 h / 23 - 70 °C / Inert atmosphere

17.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 23 °C

18.1: triethylamine; HATU / N,N-dimethyl-formamide / 14 h / 23 °C / Inert atmosphere

19.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 23 °C / Inert atmosphere

With 1H-imidazole; methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; 2-methyl-but-2-ene; Trimethyl borate; tributyl-amine; trimethylamine-N-oxide; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium hexamethylsilazane; potassium hydrogencarbonate; triethylamine; HATU; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; decane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene; 1.1: Corey-Bakshi-Shibata reduction / 4.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281