4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

Base Information

Chemical Name:4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one
CAS No.:1428771-51-0
Molecular Formula:C₂₇H₂₅O₄P
Molecular Weight:444.467
Hs Code.:

Synonyms:4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

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Chemical Property of 4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

Chemical Property:

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Technology Process of 4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

There total 3 articles about 4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1428771-48-5
C₂₆H₂₃O₄P

: 420-37-1
trimethoxonium tetrafluoroborate

: 1428771-51-0
4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

Guidance literature:: In dichloromethane; at 20 ℃; for 24h; regioselective reaction;
DOI:10.1016/j.tet.2013.03.004

Reference yield:

: 22621-30-3
4-hydroxy-5,5-dimethyl-5H-furan-2-one

: 1428771-51-0
4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 16.33 h / Reflux; Heating

2: dichloromethane / 24 h / 20 °C

In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.03.004

Reference yield:

: 73818-55-0,15596-07-3
Bestmann ylide

: 1428771-51-0
4-methoxy-5,5-dimethyl-3-[2-(triphenylphosphoranylidene)acetyl]furan-2(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 16.33 h / Reflux; Heating

2: dichloromethane / 24 h / 20 °C

In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.03.004