(propoxy-4 phenyl)-3 propenethioate de O-ethyl (E)

Base Information

• Chemical Name: (propoxy-4 phenyl)-3 propenethioate de O-ethyl (E)
• CAS No.: 125575-25-9
• Molecular Formula: C₁₄H₁₈O₂S
• Molecular Weight: 250.362
• Mol file: 125575-25-9.mol

Synonyms:(propoxy-4 phenyl)-3 propenethioate de O-ethyl (E)

Chemical Property of (propoxy-4 phenyl)-3 propenethioate de O-ethyl (E)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (propoxy-4 phenyl)-3 propenethioate de O-ethyl (E)

There total 1 articles about (propoxy-4 phenyl)-3 propenethioate de O-ethyl (E) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

O-Ethyl thioacetate (926-67-0) + 4-propoxybenzaldehyde (5736-85-6) → (propoxy-4 phenyl)-3 propenethioate de O-ethyl (E) (125575-25-9)

Guidance literature:

With sodium; In ethanol; for 21h;

DOI:10.1016/0223-5234(89)90088-3

Reference yield: 77.0%

(propoxy-4 phenyl)-3 propenethioate de O-ethyl (E) (125575-25-9) → chlorure de propoxy-4 cinnamamidinium monohydrate

Guidance literature:

With ammonia; ammonium chloride; In ethanol; for 14h; Heating;

DOI:10.1016/0223-5234(89)90088-3

Reference yield:

(propoxy-4 phenyl)-3 propenethioate de O-ethyl (E) (125575-25-9) → 2C16H27N3O*2ClH*H2O

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / NH₄Cl, NH₃ / ethanol / 14 h / Heating

2: 62 percent / ethanol / 6.5 h / Heating

With ammonia; ammonium chloride; In ethanol;

DOI:10.1016/0223-5234(89)90088-3

upstream raw materials:

O-Ethyl thioacetate

4-propoxybenzaldehyde

Refernces