N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

Base Information

Chemical Name:N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide
CAS No.:137888-43-8
Molecular Formula:C₃₆H₅₄N₈O₈S₂
Molecular Weight:791.006
Hs Code.:

Synonyms:N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

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Chemical Property of N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

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Technology Process of N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

There total 2 articles about N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 6968-11-2
N,N'-bis(benzyloxycarbonyl)-L-cystine

: 108081-89-6
glycine-3-dimethylaminopropylamide

: 137888-43-8
N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

Guidance literature:: N,N'-bis(benzyloxycarbonyl)-L-cystine; glycine-3-dimethylaminopropylamide; With polystyrene beads containing di-imide residues; benzotriazol-1-ol; In chloroform; at 25 ℃; for 16h;

With polystryrene anion-exchange beads containing quaternary ..; In dichloromethane; at 25 ℃; for 3h;
DOI:10.1016/S0040-4039(02)00064-3

Reference yield:

: 6968-11-2
N,N'-bis(benzyloxycarbonyl)-L-cystine

: glycine-3-dimethyl aminopropylamide ditrifluoroacetate

: 137888-43-8
N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

: C₃₆H₅₄N₈O₈S₃

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 24h; Product distribution; reaction under var. conditions;
DOI:10.1016/S0040-4039(00)73228-X

Reference yield:

: 137888-43-8
N,N'-bis(benzyloxycarbonyl)-L-cysteinylglycyl-3-dimethylaminopropylamide disulfide

: C₃₆H₅₄N₈O₈S₃

: C₃₆H₅₄N₈O₈S₄

: C₃₆H₅₄N₈O₈S₅

Guidance literature:: With sulfur; ammonium hydroxide; In carbon disulfide; ethanol; chloroform; for 2h; Ambient temperature;
DOI:10.1016/S0040-4039(00)73228-X