N-acetyl carbamazepine

Base Information

Chemical Name:N-acetyl carbamazepine
CAS No.:26689-55-4
Molecular Formula:C₁₇H₁₄N₂O₂
Molecular Weight:278.31
Hs Code.:

Synonyms:N-acetyl carbamazepine

Suppliers and Price of N-acetyl carbamazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N-acetyl carbamazepine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-acetyl carbamazepine

There total 1 articles about N-acetyl carbamazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 256-96-2
dibenzoazepine

: 3998-25-2
acetyl isocyanate

: 26689-55-4
N-acetyl carbamazepine

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/jps.21952

Reference yield:

: 26689-55-4
N-acetyl carbamazepine

: 298-46-4
carbamazepin

: 256-96-2
dibenzoazepine

Guidance literature:: at 70 ℃; pH=4; pH-value; Kinetics; aq. buffer;
DOI:10.1002/jps.21952

Reference yield:

: 26689-55-4
N-acetyl carbamazepine

: 298-46-4
carbamazepin

Guidance literature:: Multi-step reaction with 6 steps

1.1: 70 °C / pH 7 / aq. buffer

2.1: tetrahydrofuran / 4 h / 20 °C

3.1: sodiumsulfide nonahydrate; water / tetrahydrofuran; 1,4-dioxane / 2 h / 0 °C

4.1: dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 6 h / 0 °C / Inert atmosphere

5.1: methylhydrazine / tetrahydrofuran / -80 °C / Inert atmosphere

5.2: 24 h / 20 °C

6.1: 25 °C / pH 3 / aq. buffer

With sodiumsulfide nonahydrate; water; dicyclohexyl-carbodiimide; methylhydrazine; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1002/jps.21952