[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

Base Information

Chemical Name:[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone
CAS No.:213389-46-9
Molecular Formula:C₂₁H₁₅Cl₂NO₃
Molecular Weight:400.261
Hs Code.:

Synonyms:[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

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Chemical Property of [2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

Chemical Property:

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Technology Process of [2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

There total 7 articles about [2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 213389-45-8
3-(3-chloro-phenyl)-5-[2-(4-chloro-phenyl)-[1,3]dioxolan-2-yl]-7-methoxy-benzo[c]isoxazole

: 213389-46-9
[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

Guidance literature:: With hydrogenchloride; hydrogen; platinum on activated charcoal; In tetrahydrofuran;
DOI:10.1016/S0960-894X(03)00180-X

Reference yield:

: 91-23-6
2-Nitroanisole

: 213389-46-9
[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: AlCl₃ / CH₂Cl₂

2: K₂CO₃ / acetonitrile

3: APTS / toluene

4: 27 percent / NaOH / methanol

5: 84 percent / H₂; aq. HCl / Pt/C / tetrahydrofuran

With hydrogenchloride; sodium hydroxide; aluminium trichloride; hydrogen; potassium carbonate; 8-aminopyrene-1,3,6-trisulfonic acid, trisodium salt; platinum on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile; 1: Friedel-Crafts reaction;
DOI:10.1016/S0960-894X(03)00180-X

Reference yield:

: 766-84-7
3-chloro-benzonitrile

: 213389-46-9
[2-amino-5-(4-chloro-benzoyl)-3-methoxy-phenyl]-(3-chloro-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / NaOH / methanol

2: 84 percent / H₂; aq. HCl / Pt/C / tetrahydrofuran

With hydrogenchloride; sodium hydroxide; hydrogen; platinum on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00180-X