4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

Base Information

Chemical Name:4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate
CAS No.:150047-94-2
Molecular Formula:C₂₈H₂₄F₅NO₅
Molecular Weight:549.494
Hs Code.:

Synonyms:4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

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Chemical Property of 4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

Chemical Property:

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Technology Process of 4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

There total 8 articles about 4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132-64-9,214827-48-2
dibenzofuran

: 150047-94-2
4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) s-BuLi, TMEDA, 2.) I₂ / 1.) Et₂O, cyclohexane, RT, 24 h, 2.) Et₂O, cyclohexane, RT, 12 h

2: 93 percent / tri-o-tolylphosphine, palladium(II) acetate, Et₃N / dimethylformamide / 0.5 h / 95 °C

3: ethanol. NaOH / 2 h / Heating

4: H₂ / 10percent Pd-C / H₂O / 4 h / 2585.7 - 2844.3 Torr / Ambient temperature

5: 9 percent / 3A molecular sieves / 50 h / Heating

6: 75 percent / diphenylphosphonic azide, Et₃N / 24 h / Heating

7: ethanol. NaOH / 2 h / Heating

8: DCC / ethyl acetate / 14 h / Ambient temperature

With sodium hydroxide; N,N,N,N,-tetramethylethylenediamine; 3 A molecular sieve; diphenyl phosphoryl azide; hydrogen; iodine; sec.-butyllithium; palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tris-(o-tolyl)phosphine; palladium on activated charcoal; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 137959-93-4
3,3'-Diiododiphenylene oxide

: 150047-94-2
4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / tri-o-tolylphosphine, palladium(II) acetate, Et₃N / dimethylformamide / 0.5 h / 95 °C

2: ethanol. NaOH / 2 h / Heating

3: H₂ / 10percent Pd-C / H₂O / 4 h / 2585.7 - 2844.3 Torr / Ambient temperature

4: 9 percent / 3A molecular sieves / 50 h / Heating

5: 75 percent / diphenylphosphonic azide, Et₃N / 24 h / Heating

6: ethanol. NaOH / 2 h / Heating

7: DCC / ethyl acetate / 14 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; diphenyl phosphoryl azide; hydrogen; palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; tris-(o-tolyl)phosphine; palladium on activated charcoal; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 137959-94-5
(E)-3-[6-((E)-2-Ethoxycarbonyl-vinyl)-dibenzofuran-4-yl]-acrylic acid ethyl ester

: 150047-94-2
4-(N-tert-butyloxycarbonyl-2-aminoethyl)-6-dibenzofuranpentafluorophenylpropionate

Guidance literature:: Multi-step reaction with 6 steps

1: ethanol. NaOH / 2 h / Heating

2: H₂ / 10percent Pd-C / H₂O / 4 h / 2585.7 - 2844.3 Torr / Ambient temperature

3: 9 percent / 3A molecular sieves / 50 h / Heating

4: 75 percent / diphenylphosphonic azide, Et₃N / 24 h / Heating

5: ethanol. NaOH / 2 h / Heating

6: DCC / ethyl acetate / 14 h / Ambient temperature

With sodium hydroxide; 3 A molecular sieve; diphenyl phosphoryl azide; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In water; ethyl acetate;