diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

Base Information

• Chemical Name: diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate
• CAS No.: 1039759-55-1
• Molecular Formula: C₄₉H₅₈N₃O₉P
• Molecular Weight: 863.988

Synonyms:diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

Chemical Property of diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

Chemical Property:

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Technology Process of diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

There total 1 articles about diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

diethyl 1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate (91726-12-4,84891-34-9) + N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosine (1039759-54-0) → diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate (1039759-55-1)

Guidance literature:

With 2,4,6-trimethyl-pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 25 ℃;

DOI:10.1016/j.bmcl.2007.11.130

Reference yield: 78.3%

diethyl N-(N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosyl)-1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate (1039759-55-1) → diethyl N-(L-isoleucyl-L-tyrosyl)-1-amino-2-(4-hydroxyphenyl)ethyl phosphonate (1039759-56-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 25 ℃;

DOI:10.1016/j.bmcl.2007.11.130

upstream raw materials:

diethyl 1-amino-2-(4-benzyloxyphenyl)ethyl phosphonate

N-benzyloxycarbonyl-L-isoleucyl-O-benzyl-L-tyrosine

Downstream raw materials:

diethyl N-(L-isoleucyl-L-tyrosyl)-1-amino-2-(4-hydroxyphenyl)ethyl phosphonate

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