β-(2,2'-Dimethylbenzhydryl)glutaric acid

Base Information

Chemical Name:β-(2,2'-Dimethylbenzhydryl)glutaric acid
CAS No.:172876-76-5
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

Synonyms:β-(2,2'-Dimethylbenzhydryl)glutaric acid

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Chemical Property of β-(2,2'-Dimethylbenzhydryl)glutaric acid

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Technology Process of β-(2,2'-Dimethylbenzhydryl)glutaric acid

There total 7 articles about β-(2,2'-Dimethylbenzhydryl)glutaric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 172876-75-4
β-(2,2'-Dimethylbenzhydryl)glutaronitrile

: 172876-76-5
β-(2,2'-Dimethylbenzhydryl)glutaric acid

Guidance literature:: With potassium hydroxide; In ethylene glycol; Heating;
DOI:10.1071/CH9951707

Reference yield:

: 172876-74-3
2-(2,2'-Dimethylbenzhydryl)propane-1,3-diol bismethanesulfonate

: 151-50-8
potassium cyanide

: 172876-76-5
β-(2,2'-Dimethylbenzhydryl)glutaric acid

Guidance literature:: With N,N-dimethyl-formamide; potassium iodide; Erhitzen des Reaktionsprodukts mit NaOH in Aethylenglykol;
DOI:10.1021/ja01133a006 DOI:10.1021/ja01583a054

Reference yield:

: 172876-73-2
2-(2,2'-Dimethylbenzhydryl)propane-1,3-diol

: 172876-76-5
β-(2,2'-Dimethylbenzhydryl)glutaric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine

2: 79 percent / KI / ethanol; dimethylformamide

3: 96 percent / aq. KOH / ethane-1,2-diol / Heating

With pyridine; potassium hydroxide; potassium iodide; In ethanol; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1071/CH9951707