2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

Base Information

Chemical Name:2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene
CAS No.:880649-07-0
Molecular Formula:C₂₉H₃₆O
Molecular Weight:400.604
Hs Code.:

2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5<sup>(10)</sup>-triene

Synonyms:2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

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Chemical Property of 2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

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Technology Process of 2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

There total 1 articles about 2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 767352-09-0
2-ethyl-3-O-benzyl-estrone

: 4736-60-1
ethyltriphenylphosphonium iodide

: 880649-07-0
2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

Guidance literature:: ethyltriphenylphosphonium iodide; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 100 ℃; for 0.25h;

2-ethyl-3-O-benzyl-estrone; In dimethyl sulfoxide; mineral oil; at 100 ℃; for 16h;
DOI:10.1021/jm200483x

Reference yield: 85.0%

: 880649-07-0
2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

: 1311311-72-4
2-ethyl-3-O-benzyl-17β-(1-hydroxyethyl) estra-[1,3,5]-triene

Guidance literature:: 2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene; With borane tetrahydrofuran; In tetrahydrofuran; at 20 ℃; for 14h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; for 2h;

Reference yield: 48.0%

: 880649-07-0
2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene

: 880649-08-1
2-ethyl-3-O-benzyl-17β-(1-hydroxyethyl)estra-1,3,5(10)-triene

Guidance literature:: 2-ethyl-3-O-benzyl-17-ethylideneestra-1,3,5⁽¹⁰⁾-triene; With borane-THF; In tetrahydrofuran; at 20 ℃; for 14h;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; for 2h;
DOI:10.1021/jm200483x