C₁₃H₁₄BrNO₄

Base Information

Chemical Name:C₁₃H₁₄BrNO₄
CAS No.:1271773-59-1
Molecular Formula:C₁₃H₁₄BrNO₄
Molecular Weight:328.162
Hs Code.:

C<sub>13</sub>H<sub>14</sub>BrNO<sub>4</sub>

Synonyms:C₁₃H₁₄BrNO₄

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Chemical Property of C₁₃H₁₄BrNO₄

Chemical Property:

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Technology Process of C₁₃H₁₄BrNO₄

There total 3 articles about C₁₃H₁₄BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1271773-56-8
C₁₃H₁₅BrO₅

: 1271773-59-1
C₁₃H₁₄BrNO₄

Guidance literature:: C₁₃H₁₅BrO₅; With triethylamine; In benzene; at 20 ℃; Inert atmosphere;

With diphenyl phosphoryl azide; In benzene; at 20 ℃; Reflux; Inert atmosphere;

Reference yield:

: 1271773-53-5
C₁₅H₁₉BrO₅

: 1271773-59-1
C₁₃H₁₄BrNO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / 1,4-dioxane / 5 h / 20 °C / Heating; Reflux

1.2: 20 °C

2.1: trifluoroacetic anhydride / 0 - 20 °C / Inert atmosphere

2.2: 20 °C

3.1: triethylamine / benzene / 20 °C / Inert atmosphere

3.2: 20 °C / Reflux; Inert atmosphere

With water; triethylamine; trifluoroacetic anhydride; sodium hydroxide; In 1,4-dioxane; benzene;

Reference yield:

: 1271777-58-2
C₁₁H₁₁BrO₅

: 1271773-59-1
C₁₃H₁₄BrNO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic anhydride / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: triethylamine / benzene / 20 °C / Inert atmosphere

2.2: 20 °C / Reflux; Inert atmosphere

With triethylamine; trifluoroacetic anhydride; In benzene;