methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

Base Information

Chemical Name:methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate
CAS No.:1236182-14-1
Molecular Formula:C₂₇H₃₉N₃O₇
Molecular Weight:517.623
Hs Code.:

Synonyms:methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

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Chemical Property of methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

Chemical Property:

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Technology Process of methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

There total 1 articles about methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S,E)-methyl 4-amino-5-methylhex-2-enoate

: 1236182-08-3
(S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoic acid

: 1236182-14-1
methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101252y

Reference yield: 91.0%

: 1236182-14-1
methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate

: 1236182-19-6
C₂₆H₃₇N₃O₇

Guidance literature:: methyl (S,E)-4-((S,E)-2-(benzyloxycarbonylamino)-6-(tert-butoxycarbonylamino)hex-3-enoylamino)-5-methylhex-2-enoate; With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; water; ethyl acetate; at 0 ℃; pH=3; Inert atmosphere;
DOI:10.1021/ol101252y