[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

Base Information

Chemical Name:[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid
CAS No.:470473-70-2
Molecular Formula:C₃₅H₃₉Cl₃N₄O₈
Molecular Weight:750.076
Hs Code.:

[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

Synonyms:[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

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Chemical Property of [allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

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Technology Process of [allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

There total 5 articles about [allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 470473-86-0
[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

: 470473-70-2
[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

Guidance literature:: With lithium hydroxide; calcium chloride; In water; isopropyl alcohol; at 20 ℃; for 6h;
DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

: 172405-21-9
methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

: 470473-70-2
[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / triethylamine / CH₂Cl₂ / 0 °C

2: 90 percent / LiOH / H₂O; dioxane / 3 h / 20 °C

3: 89 percent / isobutyl chloroformate; N-methyl morpholine / CH₂Cl₂ / 1 h / -15 °C

4: 91 percent / LiOH; CaCl₂ / propan-2-ol; H₂O / 6 h / 20 °C

With 4-methyl-morpholine; lithium hydroxide; triethylamine; calcium chloride; isobutyl chloroformate; In 1,4-dioxane; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 470473-70-2
[allyloxycarbonyl-(2-{2-[(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-(2,2,2-trichloro-ethoxycarbonyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 1 h / -40 - -25 °C

2: 97 percent / triethylamine / CH₂Cl₂ / 0 °C

3: 90 percent / LiOH / H₂O; dioxane / 3 h / 20 °C

4: 89 percent / isobutyl chloroformate; N-methyl morpholine / CH₂Cl₂ / 1 h / -15 °C

5: 91 percent / LiOH; CaCl₂ / propan-2-ol; H₂O / 6 h / 20 °C

With 4-methyl-morpholine; lithium hydroxide; triethylamine; calcium chloride; isobutyl chloroformate; In 1,4-dioxane; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/S0040-4020(02)00527-6